TRACES

TRACES répond aux enjeux sociétaux de demain, en adéquation avec le concept One Health, et lève les nombreux verrous de l’analyse de traces de micropolluants dans les milieux complexes environnementaux.

Axes de recherche

Notre expertise nous permet d’appréhender l’analyse dans sa globalité : de l’échantillonnage et la préparation de l’échantillon jusqu’à l’identification et la quantification par spectrométrie de masse, en passant par la séparation chromatographique. Les méthodologies originales que nous concevons nous permettent de relever de multiples challenges tels que :

  • Etendre la gamme des composés analysables : des apolaires aux ultra-polaires
  • Abaisser les seuils de détection (< 0,01 ng/L ≡ < 10-13 mol/L)
  • Identifier et quantifier des polluants d’intérêts émergents et des composés inconnus (métabolites, produits de transformation ou de dégradation)

Nos stratégies, basées sur des analyses sélectives ou globales par spectrométrie de masse de matrices environnementales complexes (aqueuses, solides, biote), visent à caractériser et quantifier ces marqueurs de pollution chimique et mesurer leur impact sur des organismes dits sentinelles. Nous veillons également à réduire au maximum l’empreinte environnementale de l’analyse.

Projets de recherche

MIXTOX : Evaluation des impacts écotoxicologiques de cocktails de produits phytosanitaires dans les sols agricoles

Financement ADEME. Durée 36 mois. Partenaires : INRAe UMR EcoSys (porteur), Equipes Ecotoxicologie et Science du sol, Versailles INRAE – Université d’Avignon, UMR EMMAH, AvignonCNRS – Université de Franche-Comté, UMR Chrono-Environnement, Besançon

Ce projet vise à produire des connaissances nouvelles concernant la qualité des sols, en caractérisant de manière réaliste l’exposition des milieux traités et non traités par les pesticides ainsi que l’exposition des organismes, et en évaluant les effets indésirables sur la biodiversité et les fonctions écologiques associées.

L’équipe TRACES développera les outils permettant d’évaluer la contamination en pesticides des sols échantillonnés , ainsi que des vers de terre et carabes collectés dans la zone d’étude, par un screening large sans a priori. Dans un second temps, des protocoles analytiques spécifiques et sensibles seront optimisés pour quantifier les molécules sélectionnées par LC-MS/MS et GC-MS dans ces matrices.


PESPOT : Occurrence de pesticides ultra-polaires et de leurs produits de transformation dans les eaux potables

Financement Office Français de la Biodiversité, dans le cadre de « l’Appel à projets national sur le plan Ecophyto II+ ». Durée 36 mois.

Partenaires : ANSES – Laboratoire d’Hydrologie de Nancy, Nancy – SUEZ, CIRSEE, Le Pecq

Ce projet a pour objectif de caractériser des molécules mobiles, organiques et persistantes (PMOCs) dans les réseaux d’eau potables ainsi que de renseigner leurs dynamiques au cours du procédé de potabilisation. Il cible plus particulièrement les pesticides, leurs produits de dégradation, ainsi que les résidus d’oxydation qui auraient pu être formés entre l’eau brute et l’eau traitée. En effet, ces molécules ne sont actuellement pas contrôlées dans le cadre des suivis règlementaires car trop polaires pour les méthodes conventionnelles, et le recul scientifique en terme de toxicité ou de dynamique est donc actuellement très faible. Ce projet vise à apporter des connaissances sur ces contaminants de préoccupation émergente, et permettra aux gestionnaires de l’eau de mieux estimer la vulnérabilité des leurs usines face aux activités agricoles attenantes.

Dans ce projet, l’équipe TRACES développe de nouveaux outils d’échantillonnage passif (Chemcatchers) nécessaires à la caractérisation des contaminants ultra-polaires d’intérêt dans les eaux brutes et traitées. Cette caractéristique des PMOCs ne permet pas leur analyse avec des méthodes conventionnelles basées sur la RPLC et une méthode HILIC semble plus adaptée. Ainsi, suite à un premier travail de référencement des molécules pertinentes, l’équipe est en charge de développer une méthode de séparation adaptée afin de les identifier via des approches de criblage de suspects par HILIC-HRMS.

 


BIOSYSMO : Bioremediation systems exploiting synergies for improved removal of mixed pollutants 

Financement Horizon Europe. Durée 48 mois.

Partenaires : IDENER Research & Development Agrupacion de Interes Economico, Espagne – UBU Universidad de Burgos, Espagne – JSI Institut Jozef Stefan, Slovénie – LEITAT Acondicionamiento Tarrasense Associacion, Espagne – UBFC Université Bourgogne Franche Comté, France – Imperial College of Science Technology and Medicine, Angleterre – BSY Blue Synergy SL, Espagne – CIIMAR Centro Interdisciplinar de Investigacao Marinha e Ambiental, Portugal – UPM Universidad Politecnica de Madrid, Espagne – AXIA Axia Innovation UG, Allemagne – TAUW GMBH, TAUW Belgie NV, TAUW Iberia SA, TAUW Allemagne, Belgique, Espagne – EXELISIS Exelisis IKE, Grèce

Le projet BIOSYSMO a pour but de concevoir et optimiser des biosystèmes synergiques résultant de combinaisons de bactéries, de champignons et de plantes pour la dégradation et la séquestration des contaminants mixtes des sols, sédiments et eaux pollués. L’optimisation sera assistée par ordinateur afin d’obtenir les combinaisons les plus efficaces.

Dans ce projet l’équipe TRACES a pour missions le développement de méthodes permettant d’évaluer la contamination de certains sites, d’étudier la dégradation des micropolluants ciblés par microLC-MS/MS et GC-MS, et d’identifier les éventuels produits de dégradations résiduels issus des traitements de bioremédiation dans les sols et eaux pollués.

 


SERIOUS: Social and environmental risk factors in the emergence of mosquito-borne diseases in urban areas

Financement ANR. Durée 48 mois.

Partenaires : CNRS, INRAe, Univ Lyon 1, VetAgroSup, Laboratoire d’Ecologie Microbienne (LEM), UMR 5557, Villeurbanne – Laboratoire Environnement, Ville et Société (EVS), UMR 5600, Lyon – INRAe, Univ Lyon 1, EPHE, Infection Virales Pathologies Comparées (IFPC), UMR 754, Lyon – Laboratoire d’Informatique en Image et Systèmes d’Information (LIRIS), UMR 5205, Villeurbanne

Le projet SERIOUS a pour but d’évaluer si la présence du moustique tigre en ville est associée à des caractéristiques spécifiques en termes de composition chimique et microbienne des gîtes larvaires et si ces conditions modulent le microbiote associé aux larves, le développement larvaire et/ou la sélection des sites de reproduction par les femelles.

Dans ce projet, l’équipe TRACES est en charge de mettre au point et appliquer des méthodes d’analyse exhaustives des molécules organiques présentes dans les eaux des gites larvaires. Différentes méthodes d’extraction seront testées en vue de screening suspect et non ciblé par spectrométrie de masse haute résolution (HRMS).

 


DISCONNECT : Désimperméabilisation et infiltration des eaux pluviales dans des sols urbains – Mobilité des contaminants organiques et non-organiques vers la nappe et évaluation des conséquences de leur transfert

Financement ANR. Durée 24 mois.

Partenaires : CNRS, ENTPE, Univ Lyon 1, Laboratoire d’Ecologie des Hydrosystèmes Naturels et Anthropisés (LEHNA), UMR 5023, Villeurbanne – INSA Lyon, Univ Lyon 1, Déchets, Eaux, Environnement, Pollutions (DEEP), EA 7429, Villeurbanne – GRAIE, pôle Eau et Territoires, Villeurbanne

Le projet DISCONNECT vise à étudier les transferts et les impacts des polluants organiques et inorganiques liés à l’infiltration des eaux pluviales vers/sur les aquifères phréatiques, en considérant la nature et la qualité des sols traversés, souvent enrichis en métaux et autres substances organiques.

Dans ce projet, l’équipe TRACES assure la caractérisation en micropolluants organiques des lixiviats et sols afin d’évaluer les transferts, notamment les Hydrocarbures Aromatiques Polycycliques (HAP). Elle développe et est également en charge du suivi des nappes phréatiques par échantillonnage passif.

 


PC Aquathèque :

Projet ciblé du PEPR One Water Eau Bien Commun

Partenaires : Univ Lyon 1,Université Grenoble-Alpes, Université Bordeaux, Université de Toulouse, Université de Strasbourg, BRGM, CNRS, INRAE, IRD, IFREMER, Université de Rennes, Université de Montpellier, MétéoFrance

L’objectif de ce projet ciblé est de réfléchir à la mise en place de méthodes et de procédures pour collecter, archiver, conserver et rendre disponibles des échantillons d’eau et leurs analyses pour les différents acteurs de l’eau mais aussi pour les générations futures ; ces échantillons pouvant être réanalysés ultérieurement avec de nouvelles méthodes chimiques, physiques, biologiques, biochimiques ou statistiques. En s’appuyant sur une analyse des différentes réalisations existantes pour des échantillons environnementaux, puis d’un test à l’échelle de pilotes de laboratoires des solutions identifiées, le projet pourrait aboutir à un cahier des charges pour la réalisation d’une aquathèque à visée nationale, avec un mode de fonctionnement pérenne, un modèle économique soutenable sur le long terme, et s’inscrivant dans une démarche de développement durable. Les banques d’échantillons et de données représentent des outils puissants d’évaluation des mesures de recherche et des politiques de gestion/remédiation qui ont pour objectif d’anticiper les impacts futurs des changements globaux sur les socio-hydrosystèmes et d’assurer l’adaptabilité et la résilience des socio-hydrosystèmes.


VENDETTA : Réacteur d’antibiorésistance : rôle des bivalves dans la production, la dissémination et la surveillance de l’antibiorésistance dans le milieu aquatique

Financement ANSES. Durée 36 mois.

Partenaires : Université de Reims, UMR-I 02 SEBIO Unité Stress Environnementaux et BIOsurveillance des milieux aquatiques UFR Sciences Exactes et Naturelles (porteur), Université de Lorraine UMR CNRS 7564 LCPME Nancy

Le projet VENDETTA vise à étudier les interactions entre un mollusque bivalve, Dreissena polymorpha, et les acteurs de l’antibiorésistance (ATBr) (Antibiotiques, bactéries, Eléments Génétiques Mobiles) afin de mieux appréhender le rôle potentiel de la faune sauvage comme bioréacteur favorisant la dissémination de l’Antibiorésistance dans l’environnement mais également son intérêt potentiel pour surveiller l’ATBr au sein des milieux aquatiques ainsi que la toxicité potentielle des éléments associés à l’ATBr chez les organismes aquatiques.

La caractérisation des acteurs de l’antibiorésistance s’appuiera sur le développement de méthodes analytiques miniaturisées capables d’atteindre des concentrations en antibiotiques issus d’une large gamme de propriétés physico-chimiques, de l’ordre du ng/L pour les eaux de rivières et de la centaine de pg/g à l’échelle d’un individu de dreissène par LC-MS/MS.

Un intérêt particulier sera apporté à la réduction de l’impact écologique de l’analyse en diminuant la consommation de solvant sans perte de sensibilité, par un transfert de méthode des principaux antibiotiques visés et leurs métabolites vers la µLC-MS/MS.

 

Capacités expérimentales et instrumentales

Couplages

  • 3 LC-MS/MS

API4000 QTRAP couplé à une chaine Agilent

5500 QTrap couplé à une chaine Agilent

Xevo TQ-S couplé à une chaine Waters

  • 2 LC-HRMS

microToF QII couplé à une chaine Thermo

MaXIS Plus couplé à une chaine Thermo UHPLC ou nanoLC

  • GC-HRMS

Exactive GC couplé à une chaine Thermo

 

Préparation d’échantillons 

ASE 350

GenoGrinder

3 automates d’extraction : 2 Rapid Trace Zymarket et 1 AutoTrace 280

Personnels

  • Chercheurs et enseignants-chercheurs

    • Emmanuelle VULLIET
  • Soutien à la recherche

    • Gaëlle DANIELE
    • Aurélie FILDIER
    • Barbara GIROUD
    • Florent LAFAY
    • Laure WIEST
    • Guilhem ZERBINI
  • Doctorants

    • Mathilde DUNY
    • Louise DURAND
  • Ingénieur contractuel

    • Vincent DUFOUR
  • Autres

    • Lucie PINASSEAU

Publications (sources HAL)

Articles dans une revue

  • Mathilde Duny, Aurélie Cortéjade, Laure Wiest, Mickael Nicolas, Emmanuelle Vulliet. Single injection LC-MS/MS analytical method for the quantification of diverse families of micropollutants, including PFAS and organotins, in Gammarus fossarum. Journal of Chromatography A, 2024, 1720, pp.464778. ?10.1016/j.chroma.2024.464778?. ?hal-04487451?
  • Juliane Hollender, Emma L. Schymanski, Lutz Ahrens, Nikiforos Alygizakis, Frederic Béen, et al.. NORMAN guidance on suspect and non-target screening in environmental monitoring. Environmental Science Europe, 2023, 35 (1), 75 (61p.). ?10.1186/s12302-023-00779-4?. ?hal-04204173?
  • M. Lopez Viveros, S. Azimi, E. Vulliet, J. Le Roux, R. Moilleron, et al.. OBSERVER LA VILLE PAR LE PRISME DES EAUX USEES Présentation de l'Observatoire mis en oeuvre par le SIAAP en Ile de France. TSM. Techniques Sciences Méthodes – Génie urbain, génie rural, 2023, 4, pp.13-19. ?10.36904/202304013?. ?hal-04253533?
  • Léa Farouil, Yolène Duchaudé, Léa Zozo, Muriel Sylvestre, Florent Lafay, et al.. Cyclic voltammetry of immobilized particles as an alternative pesticide screening method for Aedes aegypti mosquitoes. Journal of Solid State Electrochemistry, 2023, ?10.1007/s10008-023-05398-w?. ?hal-03989889?
  • Olivier Roques, Jean-Philippe Bedell, Julia Le Maux, Laure Wiest, Christian Mougin, et al.. Assessing the Potential Ecotoxicological Risk of Different Organic Amendments Used in Agriculture: Approach Using Acute Toxicity Tests on Plants and Earthworms. Archives of Environmental Contamination and Toxicology, 2023, 84 (2), pp.248-266. ?10.1007/s00244-023-00979-2?. ?hal-04321684?
  • Corentin Mit, Anne Bado-Nilles, Cyril Turiès, Gaëlle Daniele, Barbara Giroud, et al.. PBTK-TD model of the phagocytosis activity in three-spined stickleback exposed to BPA. Aquatic Toxicology, 2023, 261, pp.106608. ?10.1016/j.aquatox.2023.106608?. ?ineris-04161285?
  • Maxime Gauthier, Jérémy Defrance, Catherine Jumarie, Emmanuelle Vulliet, Jeanne Garric, et al.. Disruption of oogenesis and molting by methoprene and glyphosate in Gammarus fossarum: involvement of retinoic acid?. Environmental Science and Pollution Research, 2023, 30 (36), pp.86060-86071. ?10.1007/s11356-023-28327-w?. ?hal-04267916?
  • Gaëlle Daniele, Florent Lafay, Carine Arnaudguilhem, Sandra Mounicou, Alain Geffard, et al.. Evaluation of the accumulation of the iodinated contrast agents diatrizoic acid and iohexol in Dreissena polymorpha mollusks. Chemosphere, 2023, 312 (1), pp.137153. ?10.1016/j.chemosphere.2022.137153?. ?hal-03870563?
  • Maxime Gauthier, Gaëlle Daniele, Barbara Giroud, Florent Lafay, Emmanuelle Vulliet, et al.. The retinoid metabolism of Gammarus fossarum is disrupted by exogenous all-trans retinoic acid, citral, and methoprene but not by the technical formulation of glyphosate. Ecotoxicology and Environmental Safety, 2023, 252, pp.114602. ?10.1016/j.ecoenv.2023.114602?. ?hal-04049321?
  • Concepcion Sanchez-Cid, Alexandre Guironnet, Christoph Keuschnig, Laure Wiest, Emmanuelle Vulliet, et al.. Gentamicin at sub-inhibitory concentrations selects for antibiotic resistance in the environment. ISME Communications, 2022, 2 (1), pp.29. ?10.1038/s43705-022-00101-y?. ?hal-03746450?
  • Emmanuelle Lebeau-Roche, Gaëlle Daniele, Aurélie Fildier, Christelle Bonnefoy, Cyril Turiès, et al.. Time and dose-dependent impairment of liver metabolism in Gasterosteus aculeatus following exposure to diclofenac (DCF) highlighted by LC-HRMS untargeted metabolomics. Science of the Total Environment, 2022, pp.159801. ?10.1016/j.scitotenv.2022.159801?. ?hal-03839504?
  • Alexandre Guironnet, Laure Wiest, Emmanuelle Vulliet. Advantages of MS/MS/MS (MRM3) vs classic MRM quantification for complex environmental matrices: Analysis of beta-lactams in WWTP sludge. Analytica Chimica Acta, 2022, 1205, pp.339773. ?10.1016/j.aca.2022.339773?. ?hal-03745350?
  • Florent Lafay, Gaëlle Daniele, Maëva Fieu, Céline Pelosi, Clémentine Fritsch, et al.. Ultrasound-assisted QuEChERS-based extraction using EDTA for determination of currently-used pesticides at trace levels in soil Authors. Environmental Science and Pollution Research, 2022, ?10.1007/s11356-022-19397-3?. ?hal-03746414?
  • Jean-Luc Bertrand-Krajewski, Rémy Bournique, Vivien Lecomte, Noémie Pernin, Laure Wiest, et al.. SIPIBEL observatory: Data on usual pollutants (solids, organic matter, nutrients, ions) and micropollutants (pharmaceuticals, surfactants, metals), biological and ecotoxicity indicators in hospital and urban wastewater, in treated effluent and sludge from wastewater treatment plant, and in surface and groundwater. Data in Brief, 2022, 40, pp.107726. ?10.1016/j.dib.2021.107726?. ?hal-03511662?
  • M Lopez Viveros, S Azimi, E Vulliet, J Le-Roux, R Moilleron, et al.. Long-term observation of the wastewater from the Parisian conurbation. Zenodo, 2022, ?10.5281/zenodo.6725353?. ?hal-04253514?
  • Melissa Lopez Viveros, Sam Azimi, Emmanuelle Vulliet, Julien Le-Roux, Régis Moilleron, et al.. Long-term observation of the end-of- treatment sludge quality from a Parisian WWTP treating wastewater from 6.5 M inhabitants. Zenodo, 2022, ?10.5281/zenodo.6724911?. ?hal-04253509?
  • Ibtissem Jlalia, Taha Chabbah, Saber Chatti, Frédéric Schiets, Hervé Casabianca, et al.. Alternating bio‐based pyridinic copolymers modified with hydrophilic and hydrophobic spacers as sorbents of aromatic pollutants. Polymers for Advanced Technologies, 2022, pp.early access. ?10.1002/pat.5578?. ?hal-03508110?
  • Alexandre Guironnet, Laure Wiest, Emmanuelle Vulliet. Improvement of the QuEChERS extraction step by matrix-dispersion effect and application on beta-lactams analysis in wastewater sludge by LC-MS/MS. Talanta, 2022, 237, pp.122923. ?10.1016/j.talanta.2021.122923?. ?hal-03508563?
  • Rania Mechichi, Taha Chabbah, Saber Chatti, Ibtissem Jlalia, Corinne Sanglar, et al.. Semi-interpenetrating Network-Coated Silica Gel Based on Green Resources for the Efficient Adsorption of Aromatic Pollutants from Waters. Chemistry Africa, In press, ?10.1007/s42250-022-00463-9?. ?hal-03772893?
  • Laure Wiest, Barbara Giroud, Maëva Fieu, Azziz Assoumani, François Lestremau, et al.. Ultrasound-assisted sample preparation for simultaneous extraction of anionic, cationic and non-ionic surfactants in sediment. Talanta, 2022, pp.123220. ?10.1016/j.talanta.2022.123220?. ?hal-03520460?
  • Corentin Mit, Anne Bado-Nilles, Gaëlle Daniele, Barbara Giroud, Emmanuelle Vulliet, et al.. The toxicokinetics of bisphenol A and its metabolites in fish elucidated by a PBTK model. Aquatic Toxicology, 2022, 247, pp.106174. ?10.1016/j.aquatox.2022.106174?. ?hal-03702730?
  • Sylvain Slaby, François Le Cor, Vincent Dufour, Lucile Auger, Laure Pasquini, et al.. Distribution of pesticides and some of their transformation products in a small lentic waterbody: Fish, water, and sediment contamination in an agricultural watershed. Environmental Pollution, 2022, 292, Part B, pp.118403. ?10.1016/j.envpol.2021.118403?. ?hal-03401371?
  • Paul Rocchi, Lucie Labied, Tristan Doussineau, Michel Julien, Barbara Giroud, et al.. Identification of Molecular Fragments in Equilibrium with Polysiloxane Ultrasmall Nanoparticles. Nanomaterials, 2022, 12 (5), pp.738. ?10.3390/nano12050738?. ?hal-03593216?
  • Emmanuelle Lebeau-Roche, Gaëlle Daniele, Aurélie Fildier, Cyril Turies, Odile Dedourge-Geffard, et al.. An optimized LC-HRMS untargeted metabolomics workflow for multi-matrices investigations in the three-spined stickleback. PLoS ONE, 2021, 16 (11), pp.e0260354. ?10.1371/journal.pone.0260354?. ?hal-03423291v2?
  • Alexandre Guironnet, Concepcion Sanchez-Cid, Timothy M. Vogel, Laure Wiest, Emmanuelle Vulliet. Aminoglycosides analysis optimization using Ion pairing Liquid Chromatography coupled to tandem Mass Spectrometry and application on wastewater samples. Journal of Chromatography A, 2021, pp.462133. ?10.1016/j.chroma.2021.462133?. ?hal-03200052?
  • Coralie Soulier, Virginie Boiteux, Patrick Candido, Emilie Caupos, Mathilde Chachignon, et al.. La spectrométrie de masse haute résolution pour la recherche de micropolluants organiques dans l’environnement. TSM. Techniques Sciences Méthodes – Génie urbain, génie rural, 2021, 6, pp.43-54. ?10.36904/tsm/202106043?. ?hal-03274374?
  • Laure Wiest, Antoine Gosset, Aurélie Fildier, Christine Libert, Matthieu Hervé, et al.. Occurrence and removal of emerging pollutants in urban sewage treatment plants using LC-QToF-MS suspect screening and quantification. Science of the Total Environment, 2021, 774, pp.145779. ?10.1016/j.scitotenv.2021.145779?. ?hal-03162034?
  • Axel Aigle, Emilie Bourgeois, Laurence Marjolet, Sabine Houot, Dominique Patureau, et al.. Spatio-temporal variations in chemical pollutants found among urban deposits match changes in thiopurine S-methyltransferase-harboring bacteria tracked by the tpm metabarcoding approach. Science of the Total Environment, 2021, 767, pp.145425. ?10.1016/j.scitotenv.2021.145425?. ?hal-03445972?
  • Sandrine Joachim, R. Beaudouin, Gaelle Daniele, A. Geffard, A. Bado-Nilles, et al.. Effects of diclofenac on sentinel species and aquatic communities in semi-natural conditions. Ecotoxicology and Environmental Safety, 2021, 211, pp.111812. ?10.1016/j.ecoenv.2020.111812?. ?hal-03113191?
  • Concepcion Sanchez-Cid, Alexandre Guironnet, Laure Wiest, Emmanuelle Vulliet, Timothy M. Vogel. Gentamicin Adsorption onto Soil Particles Prevents Overall Short-Term Effects on the Soil Microbiome and Resistome. Antibiotics, 2021, Special Issue The Distribution of Antibiotic Resistance in Terrestrial Ecosystems, 10 (2), pp.191. ?10.3390/antibiotics10020191?. ?hal-03200197?
  • Imen Abdelhadi-Miladi, Taha Chabbah, Saber Chatti, Houyem Abderrazak, Patrice Saint-Martin, et al.. Novel PDMS based semi-interpenetrating networks (IPNs) for the extraction of phenolic compounds. Journal of Environmental Chemical Engineering, 2021, 9 (1), pp.104656. ?10.1016/j.jece.2020.104656?. ?hal-03119656?
  • Ronan Guillossou, Julien Le Roux, Angélique Goffin, Romain Mailler, Gilles Varrault, et al.. Fluorescence excitation/emission matrices as a tool to monitor the removal of organic micropollutants from wastewater effluents by adsorption onto activated carbon. Water Research, 2021, 190, pp.116749. ?10.1016/j.watres.2020.116749?. ?hal-03076698?
  • Vincent Dufour, Laure Wiest, Sylvain Slaby, François Le Cor, Lucile Auger, et al.. Miniaturization of an extraction protocol for the monitoring of pesticides and polar transformation products in biotic matrices. Chemosphere, 2021, 284, pp.131292. ?10.1016/j.chemosphere.2021.131292?. ?hal-03364505?
  • Laure Wiest, Barbara Giroud, Azziz Assoumani, François Lestremau, Emmanuelle Vulliet. A multi-family offline SPE LC-MS/MS analytical method for anionic, cationic and non-ionic surfactants quantification in surface water. Talanta, 2021, 232, pp.122441. ?10.1016/j.talanta.2021.122441?. ?hal-03209496?
  • Nadine Bou Orm, Thomas Gréa, Marwa Hamandi, Alexandre Lambert, Florent Lafay, et al.. Design of Hybrid PAH Nanoadsorbents by Surface Functionalization of ZrO2 Nanoparticles with Phosphonic Acids. Nanomaterials, 2021, 11 (4), pp.952. ?10.3390/nano11040952?. ?hal-03318468?
  • Céline Pelosi, Colette Bertrand, Gaëlle Daniele, M. Coeurdassier, Pierre Benoit, et al.. Residues of currently used pesticides in soils and earthworms: A silent threat?. Agriculture, Ecosystems & Environment, 2021, 305, pp.107167. ?10.1016/j.agee.2020.107167?. ?hal-02968489?
  • Barbara Giroud, Audrey Buleté, Loïc Spinner, Julie Deverchère, Léa Payen-Gay, et al.. Quantification of the organophosphate flame retardant triphenylphosphate and its main metabolite in whole blood by liquid–liquid micro-extraction and liquid chromatography-tandem mass spectrometry. Microchemical Journal, 2021, 168, pp.106374. ?10.1016/j.microc.2021.106374?. ?hal-03318023?
  • Bastian Schulze, Denice van Herwerden, Ian Allan, Lubertus Bijlsma, Nestor Etxebarria, et al.. Inter-laboratory mass spectrometry dataset based on passive sampling of drinking water for non-target analysis. Scientific Data , 2021, 8 (1), pp.223. ?10.1038/s41597-021-01002-w?. ?hal-03325586?
  • Antoine Gosset, Laure Wiest, Aurélie Fildier, Christine Libert, Barbara Giroud, et al.. Ecotoxicological risk assessment of contaminants of emerging concern identified by “suspect screening” from urban wastewater treatment plant effluents at a territorial scale. Science of the Total Environment, 2021, 778, pp.146275. ?10.1016/j.scitotenv.2021.146275?. ?hal-03167988?
  • Dominique Patureau, Romain Mailler, Nadine Delgenes, Alice Danel, Emmanuelle Vulliet, et al.. Fate of emerging and priority micropollutants during the sewage sludge treatment - Part 2: Mass balances of organic contaminants on sludge treatments are challenging. Waste Management, 2021, 125, pp.122-131. ?10.1016/j.wasman.2021.02.034?. ?hal-03161576?
  • Gwenaëlle Corbin, Emmanuelle Vulliet, Bruno Lanson, Albert Rimola, Pierre Mignon. Adsorption of Pharmaceuticals onto Smectite Clay Minerals: A Combined Experimental and Theoretical Study. Minerals, 2021, 11 (1), pp.62. ?10.3390/min11010062?. ?hal-03135489?
  • Lucie Pinasseau, Laure Wiest, Laurence Volatier, Florian Mermillod-Blondin, Emmanuelle Vulliet. Emerging polar pollutants in groundwater: Potential impact of urban stormwater infiltration practices. Environmental Pollution, 2020, 266, pp.115387. ?10.1016/j.envpol.2020.115387?. ?hal-02971585?
  • Vincent Dufour, Laure Wiest, Sylvain Slaby, François Le Cor, Lucile Auger, et al.. Development of a simple multiresidue extraction method for the quantification of a wide polarity range list of pesticides and transformation products in eggs by liquid chromatography and tandem mass spectrometry. Journal of Chromatography A, 2020, 1628, pp.1-9. ?10.1016/j.chroma.2020.461447?. ?hal-03011261?
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  • Alice Vidal, Florent Lafay, Gaëlle Danièle, Emmanuelle Vulliet, Eric Rochard, et al.. Does water temperature influence the distribution and elimination of perfluorinated substances in rainbow trout (Oncorhynchus mykiss)?. Environmental Science and Pollution Research, 2019, 26 (16), pp.16355-16365. ?10.1007/s11356-019-05029-w?. ?hal-02140083?
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  • Hélène Arambourou, Emmanuelle Vulliet, Gaëlle Danièle, Patrice Noury, Nicolas Delorme, et al.. Comparison in the response of three European Gammarid species exposed to the growth regulator insecticide fenoxycarb. Environmental Science and Pollution Research, 2019, 26 (11), pp.11496-11502. ?10.1007/s11356-019-04631-2?. ?hal-02140086?
  • Christelle Bonnefoy, Aurélie Fildier, Audrey Buleté, Claire Bordes, Jeanne Garric, et al.. Untargeted analysis of nanoLC-HRMS data by ANOVA-PCA to highlight metabolites in Gammarus fossarum after in vivo exposure to pharmaceuticals. Talanta, 2019, 202, pp.221-229. ?10.1016/j.talanta.2019.04.028?. ?hal-02124467?
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  • A. Bergé, A. Bulete, A. Fildier, Johnny Gasperi, R. Mailler, et al.. La spectrométrie de masse haute résolution : un outil innovant de caractérisation des ouvrages d’assainissement. TSM. Techniques Sciences Méthodes – Génie urbain, génie rural, 2018, 12, pp.51-68. ?hal-01993194?
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  • Martin Sordet, Audrey Bulete, Emmanuelle Vulliet. A rapid and easy method based on hydrophilic interaction chromatography coupled with tandem mass spectrometry (HILIC-MS/MS/MS) to quantify iodinated X-ray contrast in wastewaters. Talanta, 2018, 190, pp.480-486. ?10.1016/j.talanta.2018.08.006?. ?hal-01900226?
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  • Chang He, Karin English, Christine Baduel, Phong Thai, Paul Jagals, et al.. Concentrations of organophosphate flame retardants and plasticizers in urine from young children in Queensland, Australia and associations with environmental and behavioural factors. Environmental Research, 2018, 164, pp.262-270. ?10.1016/j.envres.2018.02.040?. ?hal-01744644?
  • Laure Wiest, Teofana Chonova, Alexandre Bergé, Robert Baudot, Frédérique Bessueille-Barbier, et al.. Two-year survey of specific hospital wastewater treatment and its impact on pharmaceutical discharges. Environmental Science and Pollution Research, 2018, 25 (10), pp.9207-9218. ?10.1007/s11356-017-9662-5?. ?hal-01569749?
  • Hélène Arambourou, Inmaculada Fuertes, Emmanuelle Vulliet, Gaëlle Danièle, Patrice Noury, et al.. Fenoxycarb exposure disrupted the reproductive success of the amphipod Gammarus fossarum with limited effects on the lipid profile. PLoS ONE, 2018, 13 (4), pp.Article number e0196461. ?10.1371/journal.pone.0196461?. ?hal-01803483?
  • Asma Ennigrou, Hervé Casabianca, Emmanuelle Vulliet, Belgacem Hanchi, Karim Hosni. Assessing the fatty acid, essential oil composition, their radical scavenging and antibacterial activities of Schinus terebinthifolius Raddi leaves and twigs. Journal of Food Science and Technology-Mysore, 2018, pp.1582-1590. ?10.1007/s13197-018-3049-6?. ?hal-01770928?
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  • Gaëlle Daniele, Florent Lafay, Céline Pelosi, Clémentine Fritsch, Emmanuelle Vulliet. Development of a method for the simultaneous determination of multi-class pesticides in earthworms by liquid chromatography coupled to tandem electrospray mass spectrometry. Analytical and Bioanalytical Chemistry, 2018, 410 (20), ?10.1007/s00216-018-1151-2?. ?hal-01811624?
  • Gaëlle Daniele, Barbara Giroud, Claire Jabot, Emmanuelle Vulliet. Exposure assessment of honeybees through study of hive matrices: analysis of selected pesticide residues in honeybees, beebread, and beeswax from French beehives by LC-MS/MS. Environmental Science and Pollution Research, 2018, 25 (7), pp.6145-6153. ?10.1007/s11356-017-9227-7?. ?hal-01574982?
  • Teofana Chonova, Vivien Lecomte, Jean-Luc Bertrand-Krajewski, Agnes Bouchez, Jérôme Labanowski, et al.. The SIPIBEL project: treatment of hospital and urban wastewater in a conventional urban wastewater treatment plant.. Environmental Science and Pollution Research, 2018, 25 (10), pp.9197-9206. ?10.1007/s11356-017-9302-0?. ?hal-01606931?
  • Agnèta Kiss, Alexandre Bergé, Bruno Domenjoud, Adriana Gonzalez-Ospina, Emmanuelle Vulliet. Chemometric and high-resolution mass spectrometry tools for the characterization and comparison of raw and treated wastewater samples of a pilot plant on the SIPIBEL site. Environmental Science and Pollution Research, 2018, 25 (10), pp.9230-9242. ?10.1007/s11356-017-0748-x?. ?hal-01682862?
  • Adriana Gonzalez-Ospina, Bruno Domenjoud, Emmanuelle Vulliet, Sylvie Bony, Sylvie Baig. Oxydation biologique et chimique à l’ozone des micropolluants émergents en station d’épuration. Environnement, Risques & Santé, 2018, 17 (2), pp.75-83. ?10.1684/ers.2017.1097?. ?hal-01803518?
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  • Charlène Pouech, Laure Wiest, Florent Lafay, Didier Léonard, Cécile Cren-Olive, et al.. Méthodes analytiques pour l'étude de la migration des additifs des conditionnements plastiques pour des applications pharmaceutiques. STP PHARMA PRATIQUES : TECHNIQUES REGLEMENTATION, 2018, 28 (3&4), pp.155-165. ?hal-01915920?
  • Alexandre Bergé, Laure Wiest, Robert Baudot, Barbara Giroud, Emmanuelle Vulliet. Occurrence of multi-class surfactants in urban wastewater: contribution of a healthcare facility to the pollution transported into the sewerage system. Environmental Science and Pollution Research, 2018, 25 (10), pp.9219-9229. ?10.1007/s11356-017-0470-8?. ?hal-01682871?
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  • Philippine G.J. Granger Joly de Boissel, Patrice Gonzalez, Audrey Buleté, Guillemine Daffe, Christelle Clérandeau, et al.. An innovative and integrative assay for toxicity testing using individual fish embryos. Application to oxazepam . Chemosphere, 2017, 181, pp.468-477. ?10.1016/j.chemosphere.2017.04.067?. ?hal-01544714?
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  • Adriana Gonzalez-Ospina, Bruno Domenjoud, Emmanuelle Vulliet, Agneta Kiss, Alexandre Bergé, et al.. Élimination des composés pharmaceutiques en station d’épuration par traitements biologiques et ozonation tertiaire. TSM. Techniques Sciences Méthodes – Génie urbain, génie rural, 2016, 6, pp.45-58. ?10.1051/tsm/201606045?. ?hal-01355571?
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  • R. Mailler, J. Gasperi, Y. Coquet, C. Derome, A. Buleté, et al.. Élimination des polluants émergents dans les rejets de STEP - 2. Étude expérimentale des processus de sorption sur le charbon actif . TSM. Techniques Sciences Méthodes – Génie urbain, génie rural, 2016, 3, ?10.1051/tsm/201603028?. ?hal-01302404?
  • Laure Wiest, Emmanuelle Vulliet. Analyse multi-résidus de pesticides dans le miel : enjeux et défis analytiques. Annales des falsifications, de l'expertise chimique et toxicologique, 2016, 985, pp.17-27. ?hal-01574998?
  • Céline Becouze-Lareure, A Dembele, Marina Coquery, Cécile Cren-Olivé, B. Barillon, et al.. Source characterisation and loads of metals and pesticides in urban wet weather discharges. Urban Water Journal, 2016, 13 (6), pp.600-617. ?10.1080/1573062X.2015.1011670?. ?hal-01356456?
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  • R. Mailler, J. Gasperi, Y. Coquet, A. Buleté, E. Vulliet, et al.. Removal of a wide range of emerging pollutants from wastewater treatment plant discharges by micro-grain activated carbon in fluidized bed as tertiary treatment at large pilot scale. Science of the Total Environment, 2016, 542, ?10.1016/j.scitotenv.2015.10.153?. ?hal-01228409?
  • Charlène Pouech, Agnèta Kiss, Florent Lafay, Didier Léonard, Laure Wiest, et al.. Human exposure assessment to a large set of polymer additives through the analysis of urine by solid phase extraction followed by ultra high performance liquid chromatography coupled to tandem mass spectrometry. Journal of Chromatography A, 2015, 1423, pp.111-123. ?10.1016/j.chroma.2015.10.091?. ?hal-01241519?
  • Mikaël Tournier, Charlène Pouech, Nadia Quignot, Florent Lafay, Laure Wiest, et al.. Determination of endocrine disruptors and endogenic androgens and estrogens in rat serum by high-performance liquid chromatography–tandem mass spectrometry. Steroids, 2015, 104, pp.252-262. ?10.1016/j.steroids.2015.10.011?. ?hal-01241662?
  • Alexandre Bergé, Emmanuelle Vulliet. Development of a method for the analysis of hormones and pharmaceuticals in earthworms by quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction followed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Analytical and Bioanalytical Chemistry, 2015, 407 (26), pp.7995-8008. ?10.1007/s00216-015-8972-z?. ?hal-01229268?
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  • R. Mailler, J. Gasperi, Y. Coquet, S. Deshayes, S. Zedek, et al.. Study of a large scale powdered activated carbon pilot: Removals of a wide range of emerging and priority micropollutants from wastewater treatment plant effluents. Water Research, 2015, 72, pp.315-330. ?10.1016/j.watres.2014.10.047?. ?hal-01103115?
  • Claire Jabot, Maeva Fieu, Barbara Giroud, Audrey Buleté, Hervé Casabianca, et al.. Trace-level determination of pyrethroid, neonicotinoid and carboxamide pesticides in beeswax using dispersive solid-phase extraction followed by ultra-high-performance liquid chromatography-tandem mass spectrometry. International Journal of Environmental Analytical Chemistry, 2015, 95 (3), pp.240-257. ?10.1080/03067319.2015.1016011?. ?hal-01187328?
  • Chaouki Belgacem, Raouf Medimagh, Aurélie Fildier, Audrey Buleté, Hans R. Kricheldorf, et al.. Synthesis and characterization of isosorbide-based α,ω-dihydroxyethersulfone oligomers. Designed Monomers and Polymers, 2015, 18 (1), pp.64-72. ?10.1080/15685551.2014.947554?. ?hal-01070696?
  • Marie-Virginie Salvia, Maeva Fieu, Emmanuelle Vulliet. Determination of tetracycline and fluoroquinolone antibiotics at trace levels in sludge and soil. Applied and Environmental Soil Science, 2015, 2015, pp.article ID 435741. ?10.1155/2015/435741?. ?hal-01356467?
  • Julien Camilleri, Robert Baudot, Laure Wiest, Emmanuelle Vulliet, Cécile Cren-Olivé, et al.. Multiresidue fully automated online SPE-HPLC-MS/MS method for the quantification of endocrine-disrupting and pharmaceutical compounds at trace level in surface water. International Journal of Environmental Analytical Chemistry, 2015, 95 (1), pp.67-81. ?10.1080/03067319.2014.983494?. ?hal-01119523?
  • Nizar Ben Salah, Hervé Casabianca, Hichem Ben Jannet, Sophie Chenavas, Sanglar Corinne, et al.. Phytochemical and biological investigation of two diplotaxis species growing in Tunisia: D-virgata & D-erucoides. Molecules, 2015, 20 (10), pp.18128-18143. ?10.3390/molecules201018128?. ?hal-01356843?
  • Chaouki Belgacem, Raouf Medimagh, Aurélie Fildier, Audrey Buleté, Hans R. Kricheldorf, et al.. Synthesis and characterization of isosorbide-based alpha,omega-dihydroxyethersulfone oligomers. Designed Monomers and Polymers, 2015, 18 (1), pp.64-72. ?10.1080/15685551.2014.947554?. ?hal-01187447?
  • Alexandra Berlioz-Barbier, Robert Baudot, Laure Wiest, Marion Gust, Jeanne Garric, et al.. MicroQuEChERS-nanoliquid chromatography-nanospray-tandem mass spectrometry for the detection and quantification of trace pharmaceuticals in benthic invertebrates. Talanta, 2015, 132, pp.796-802. ?10.1016/j.talanta.2014.10.030?. ?hal-01187418?
  • Julien Camilleri, Emmanuelle Vulliet. Determination of steroid hormones in sediments based on quick, easy, cheap, effective, rugged, and safe (modified-QuEChERS) extraction followed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Analytical Methods, 2015, 7 (22), pp.9577-9586. ?10.1039/c5ay01972a?. ?hal-01241666?
  • Yannick Poquet, Laurent Bodin, Marc Tchamitchian, Marion Fusellier, Barbara Giroud, et al.. A pragmatic approach to assess the exposure of the honey bee (Apis mellifera) when subjected to pesticide spray. PLoS ONE, 2014, 9 (11), pp.Article Number: e113728. ?10.1371/journal.pone.0113728?. ?hal-01230268?
  • Alexandra Berlioz-Barbier, Audrey Buleté, Juliette Fabure, Jeanne Garric, Cécile Cren-Olivé, et al.. Multi-residue analysis of emerging pollutants in benthic invertebrates by modified micro-quick-easy-cheap-efficient-rugged-safe extraction and nanoliquid chromatography-nanospray-tandem mass spectrometry analysis. Journal of Chromatography A, 2014, 1367, pp.16-32. ?10.1016/j.chroma.2014.09.044?. ?hal-01230302?
  • Emmanuelle Vulliet, Alexandra Berlioz-Barbier, Florent Lafay, Robert Baudot, Laure Wiest, et al.. A national reconnaissance for selected organic micropollutants in sediments on French territory. Environmental Science and Pollution Research, 2014, 21, 19, pp.11370-11379. ?10.1007/s11356-014-3089-z?. ?hal-01230435?
  • Marie-Virginie Salvia, Cécile Cren-Olivé, Laure Wiest, Robert Baudot, Emmanuelle Vulliet. Comparison of Two Analytical Methods for the Determination of Traces of Veterinary Antibiotics and Steroid Hormones in Soil Based on Pressurised Liquid Extraction (PLE) and Quick, Easy, Cheap, Effective, Rugged, Safe (Modified-Quechers) Extraction. Pharmaceutica Analytica Acta, 2014, 5 (9), pp.1000315. ?10.4172/2153-2435.1000315?. ?hal-01100640?
  • Marie-Virginie Salvia, Julie Experton, Claire Geandel, Cécile Cren-Olivé, Emmanuelle Vulliet. Fate of pharmaceutical compounds and steroid hormones in soil: study of transfer and degradation in soil columns.. Environmental Science and Pollution Research, 2014, 21 (17), pp.10525-10535. ?10.1007/s11356-014-3038-x?. ?hal-01070854?
  • Raouf Medimagh, Asma Saadaoui, Salma Mghirbi, Sylvain Marque, Damien Prim, et al.. New biosourced alternated poly(ether)Ester-Amides (PeEA): synthesis and combined NMR/MALDI ToF MS characterization. Journal of Polymer Research, 2014, 21 (6), pp.article 486. ?10.1007/s10965-014-0486-4?. ?hal-01057926?
  • Emmanuelle Vulliet, Mikaël Tournier, Antoine Vauchez, Laure Wiest, Robert Baudot, et al.. Survey regarding the occurrence of selected organic micropollutants in the groundwaters of overseas departments. Environmental Science and Pollution Research, 2014, 21 (12), pp.7512-7521. ?10.1007/s11356-014-2619-z?. ?hal-01071649?
  • Raphaël Santos, M. Palos-Ladeiro, A. Besnard, Emmanuelle Vulliet, J. M. Porcher, et al.. Kinetic response of a genotoxicity biomarker in the three-spined stickleback and implication for environmental monitoring. Ecotoxicology and Environmental Safety, 2014, 102, pp.6-11. ?10.1016/j.ecoenv.2014.01.006?. ?halsde-00784680?
  • Johnny Gasperi, C. Sebastian, Véronique Ruban, M. Delamain, S. Percot, et al.. Micropollutants in urban stormwater: occurrence, concentrations, and atmospheric contributions for a wide range of contaminants in three French catchments. Environmental Science and Pollution Research, 2014, 21 (8), pp.5267-5281. ?10.1007/s11356-013-2396-0?. ?hal-00923251?
  • Gislain Lipeme Kouyi, Cécile Cren-Olivé, Benoît Cournoyer. Chemical, microbiological, and spatial characteristics and impacts of contaminants from urban catchments: CABRRES project. Environmental Science and Pollution Research, 2014, 21 (8), pp.5263-5266. ?10.1007/s11356-014-2612-6?. ?hal-00991574?
  • Haythem Bennour, Raouf Medimagh, Aurélie Fildier, Guy Raffin, Marie Hangouët, et al.. Hyperbranched cyclic and multicyclic poly(etherketone)s by polycondensation of isosorbide and isomannide with 2,6,4′-trifluorobenzophenone and 1,3,5-tris(4-fluorobenzoyl) benzene. High Performance Polymers, 2014, 26 (2), pp.144-155. ?10.1177/0954008313501912?. ?hal-00965439?
  • Agnèta Kiss, Claire Bordes, Corinne Buisson, Françoise Lasne, Pierre Lanteri, et al.. Data-handling strategies for metabonomic studies: example of the UHPLC-ESI/ToF urinary signature of tetrahydrocannabinol in humans. Analytical and Bioanalytical Chemistry, 2014, 406 (4), pp.1209-1219. ?10.1007/s00216-013-7199-0?. ?hal-00850196?
  • Charlène Pouech, Florent Lafay, Laure Wiest, Robert Baudot, Didier Léonard, et al.. Monitoring the extraction of additives and additive degradation products from polymer packaging into solutions by multi-residue method including solid phase extraction and ultra-high performance liquid chromatography-tandem mass spectrometry analysis. Analytical and Bioanalytical Chemistry, 2014, 406 (5), pp.1493-1507. ?10.1007/s00216-013-7551-4?. ?hal-00924245?
  • Alexandra Berlioz-Barbier, Antoine Vauchez, Laure Wiest, Robert Baudot, Emmanuelle Vulliet, et al.. Multi-residue analysis of emerging pollutants in sediment using QuEChERS-based extraction followed by LC-MS/MS analysis.. Analytical and Bioanalytical Chemistry, 2014, 406 (4), pp.1259-1266. ?10.1007/s00216-013-7450-8?. ?hal-00955924?
  • Raouf Medimagh, Salma Mghirbi, Asma Saadaoui, Aurélie Fildier, Marlène Desloir-Bonjour, et al.. Synthesis of biosourced polyether-amides from 1,4-3,6-dianhydrohexitols: Characterization by NMR and MALDI-ToF mass spectrometry. Comptes Rendus. Chimie, 2013, 16 (12), pp.1127-1139. ?10.1016/j.crci.2013.05.004?. ?hal-00905733?
  • Marie-Virginie Salvia, Cécile Cren-Olivé, Emmanuelle Vulliet. Statistical evaluation of the influence of soil properties on recoveries and matrix effects during the analysis of pharmaceutical compounds and steroids by quick, easy, cheap, effective, rugged and safe extraction followed by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2013, 1315, pp.53-60. ?10.1016/j.chroma.2013.09.056?. ?hal-00877918?
  • Barbara Giroud, Antoine Vauchez, Emmanuelle Vulliet, Laure Wiest, Audrey Buleté. Trace level determination of pyrethroid and neonicotinoid insecticides in beebread using acetonitrile-based extraction followed by analysis with ultra-high-performance liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 2013, 1316, pp.53-61. ?10.1016/j.chroma.2013.09.088?. ?hal-00877912?
  • Amélie Levet, Claire Bordes, Yohann Clément, Pierre Mignon, Henry Chermette, et al.. Quantitative structure-activity relationship to predict acute fish toxicity of organic solvents. Chemosphere, 2013, 93 (6), pp.1094-1103. ?10.1016/j.chemosphere.2013.06.002?. ?hal-00877400?
  • Agnèta Kiss, Marianna Lucio, Aurélie Fildier, Corinne Buisson, Philippe Schmitt-Kopplin, et al.. Doping control using high and ultra-high resolution mass spectrometry based non-targeted metabolomics-A case study of salbutamol and budesonide abuse. PLoS ONE, 2013, 8 (9), pp.e74584. ?10.1371/journal.pone.0074584?. ?hal-00865161?
  • Hana Ben Abderrazak, Aurélie Fildier, Hatem Ben Romdhane, Saber Chatti, Hans R. Kricheldorf. Synthesis of new poly(ether ketone)s derived from biobased diols. Macromolecular Chemistry and Physics, 2013, 214 (13), pp.1423-1433. ?10.1002/macp.201300015?. ?hal-00850452?
  • Raphaël Santos, M. Palos-Ladeiro, A. Besnard, J. Reggio, Emmanuelle Vulliet, et al.. Parental exposure to methyl methane sulfonate of three-spined stickleback: contribution of DNA damage in male and female germ cells to further development impairment in progeny. Ecotoxicology, 2013, 22 (5), pp.815-824. ?10.1007/s10646-013-1088-3?. ?hal-00860498?
  • Mélanie Villeret, Sabrina Jolly, Laure Wiest, Emmanuelle Vulliet, Anne Bado-Nilles, et al.. A potential biomarker of androgen exposure in European bullhead (Cottus sp.) kidney. Fish Physiology and Biochemistry, 2013, 39 (3), pp.573-580. ?10.1007/s10695-012-9720-3?. ?hal-00860752?
  • Saber Chatti, Steffen M. Weidner, Aurélie Fildier, Hans R. Kricheldorf. Copolyesters of isosorbide, succinic acid, and isophthalic acid: Biodegradable, high T-g engineering plastics. Journal of polymer science. Part A-1, Polymer chemistry, 2013, 51 (11), pp.2464-2471. ?10.1002/pola.26635?. ?hal-00993086?
  • William Peysson, Emmanuelle Vulliet. Determination of 136 pharmaceuticals and hormones in sewage sludge using quick, easy, cheap, effective, rugged and safe extraction followed by analysis with liquid chromatography-time-of-flight-mass spectrometry. Journal of Chromatography A, 2013, 1290, pp.46-61. ?10.1016/j.chroma.2013.03.057?. ?hal-00825023?
  • Angélique Lazartigues, Marielle Thomas, Damien Banas, Jean Brun-Bellut, Cécile Cren-Olivé, et al.. Accumulation and half-lives of 13 pesticides in muscle tissue of freshwater fishes through food exposure. Chemosphere, 2013, 91 (4), pp.530-535. ?10.1016/j.chemosphere.2012.12.032?. ?hal-00860781?
  • Emmanuelle Vulliet, Barbara Giroud, Pédro Marote. Determination of testosterone and its photodegradation products in surface waters using solid-phase extraction followed by LC-MS/MS analysis. Environmental Science and Pollution Research, 2013, 20 (1), pp.117-125. ?10.1007/s11356-012-1041-7?. ?hal-00993064?
  • Angélique Lazartigues, Marielle Thomas, Cécile Cren-Olivé, Jean Brun-Bellut, Yves Le Roux, et al.. Pesticide pressure and fish farming in barrage pond in Northeastern France. Part II: residues of 13 pesticides in water, sediments, edible fish and their relationships. Environmental Science and Pollution Research, 2013, 20 (1), pp.117-125. ?10.1007/s11356-012-1167-7?. ?hal-00798623?
  • Olivier Lambert, Mélanie Piroux, Sophie Puyo, Chantal Thorin, Monique L'Hostis, et al.. Widespread occurrence of chemical residues in beehive matrices from apiaries located in different landscapes of Western France.. PLoS ONE, 2013, 8 (6), pp.e67007. ?10.1371/journal.pone.0067007?. ?hal-01071820?
  • N. Morin, Julien Camilleri, Cécile Cren-Olivé, Marina Coquery, Cecile Miege. Determination of uptake kinetics and sampling rates for 56 organic micropollutants with "pharmaceutical" POCIS. Talanta, 2013, 109, p. 61 - p. 73. ?10.1016/j.talanta.2013.01.058?. ?hal-00937619?
  • Marie-Virginie Salvia, Emmanuelle Vulliet, Laure Wiest, Robert Baudot, Cécile Cren-Olivé. Development of a multi-residue method using acetonitrile-based extraction followed by liquid chromatography-tandem mass spectrometry for the analysis of steroids and veterinary and human drugs at trace levels in soil. Journal of Chromatography A, 2012, 1245, pp.122-133. ?10.1016/j.chroma.2012.05.034?. ?hal-00705807?
  • Nadia Quignot, Marine Arnaud, Franck Robidel, Anthony Lecomte, Mikaël Tournier, et al.. Characterization of endocrine-disrupting chemicals based on hormonal balance disruption in male and female adult rats. Reproductive Toxicology, 2012, 33 (3), pp.339-352. ?10.1016/j.reprotox.2012.01.004?. ?hal-00698483?
  • Nadia Quignot, Mikaël Tournier, Charlène Pouech, Cécile Cren-Olivé, Robert Barouki, et al.. Quantification of steroids and endocrine disrupting chemicals in rat ovaries by LC-MS/MS for reproductive toxicology assessment. Analytical and Bioanalytical Chemistry, 2012, 403 (6), pp.1629-1640. ?10.1007/s00216-012-5990-y?. ?hal-00727355?
  • Cécile Cren-Olivé, Audrey Buleté, Florent Rouvière, Carine Arnaudguilhem. Multiresidue analysis of aromatic organochlorines in soil by gas chromatography-mass spectrometry and QuEChERS extraction based on water/dichloromethane partitioning. Comparison with accelerated solvent extraction.. Talanta, 2012, 93, pp.336-344. ?10.1016/j.talanta.2012.02.048?. ?hal-00695768?
  • Julien Camilleri, Nicolas Morin, Cecile Miege, Marina Coquery, Cécile Cren-Olivé. Determination of the uptake and release rates of multifamilies of endocrine disruptor compounds on the polar C18 Chemcatcher. Three potential performance reference compounds to monitor polar pollutants in surface water by integrative sampling. Journal of Chromatography A, 2012, 1237, pp.37-45. ?10.1016/j.chroma.2012.03.025?. ?hal-00697815?
  • Charlène Pouech, Mikaël Tournier, Nadia Quignot, Agnèta Kiss, Laure Wiest, et al.. Multi-residue analysis of free and conjugated hormones and endocrine disruptors in rat testis by QuEChERS-based extraction and LC-MS/MS. Analytical and Bioanalytical Chemistry, 2012, 402 (9), pp.2777-2788. ?10.1007/s00216-012-5723-2?. ?hal-00727414?
  • Estelle Pujos, Cécile Cren-Olivé, Patrick Goetinck, Marie-Magdeleine Flament-Waton, Marie-Florence Grenier-Loustalot. Optimization of the extraction and analysis of natural androgen steroids and their metabolites in urine by GC/MS and GC/FID. Analytical Letters, 2012, 45 (4), pp.356-366. ?10.1080/00032719.2011.644735?. ?hal-00727420?
  • Alexandra Badiou-Bénéteau, Stephan M. Carvalho, Jean-Luc Brunet, Geraldo A. Carvalho, Audrey Buleté, et al.. Development of biomarkers of exposure to xenobiotics in the honey bee Apis mellifera: Application to the systemic insecticide thiamethoxam. Ecotoxicology and Environmental Safety, 2012, 82 (1), pp.22-31. ?10.1016/j.ecoenv.2012.05.005?. ?hal-00924275?
  • Nathalie Gineys, Barbara Giroud, Mickael Gineys, Emmanuelle Vulliet. Retention of selected steroids on a silt-loam soil.. Journal of Environmental Science and Health, Part A, 2012, 47 (13), pp.2133-2140. ?10.1080/10934529.2012.696021?. ?hal-00965997?
  • Karim Hosni, Marwa Jemli, Salma Dziri, Yacine M'Rabet, Asma Ennigrou, et al.. Changes in phytochemical, antimicrobial and free radical scavenging activities of the Peruvian pepper tree (Schinus molle L.) as influenced by fruit maturation. Industrial Crops and Products, 2011, 34 (3), pp.1622-1628. ?10.1016/j.indcrop.2011.06.004?. ?hal-00616337?
  • Camille Pasquet, Emmanuelle Vulliet. Utilisation of an enzyme-linked immunosorbent assay (ELISA) for determination of alkylphenols in various environmental matrices. Comparison with LC-MS/MS method. Talanta, 2011, 85 (5), pp.2492-2497. ?10.1016/j.talanta.2011.07.102?. ?hal-00639311?
  • Angélique Lazartigues, Cédric Fratta, Robert Baudot, Laure Wiest, Cyril Feidt, et al.. Multiresidue method for the determination of 13 pesticides in three environmental matrices: water, sediments and fish muscle. Talanta, 2011, 85 (3), pp.1500-1507. ?10.1016/j.talanta.2011.06.023?. ?hal-00616328?
  • Laure Wiest, Audrey Buleté, Barbara Giroud, Cédric Fratta, Sophie Amic, et al.. Multi-residue analysis of 80 environmental contaminants in honeys, honeybees and pollens by one extraction procedure followed by liquid and gas chromatography coupled with mass spectrometric detection. Journal of Chromatography A, 2011, 1218 (34), pp.5743-5756. ?10.1016/j.chroma.2011.06.079?. ?hal-00639315?
  • Céline Becouze, Laure Wiest, Robert Baudot, Jean-Luc Bertrand-Krajewski, Cécile Cren-Olivé. Optimisation of pressurised liquid extraction for the ultra-trace quantification of 20 priority substances from the European Water Framework Directive in atmospheric particles by GC-MS and LC-FLD-MS/MS. Analytica Chimica Acta, 2011, 693 (1-2), pp.47-53. ?10.1016/j.aca.2011.03.008?. ?hal-00592008?
  • Emmanuelle Vulliet, Cécile Cren-Olivé, Marie-Florence Grenier-Loustalot. Occurrence of pharmaceuticals and hormones in drinking water treated from surface waters. Environmental Chemistry Letters, 2011, 9 (1), pp.103-114. ?10.1007/s10311-009-0253-7?. ?hal-00509280?
  • Agnèta Kiss, Anne-Laure Jacquet, Marie-Magdeleine Flament-Waton, Jean-Olivier Païssé, Jacques de Ceaurriz, et al.. Urinary signature of anabolic steroids and glucocorticoids in humans by LC-MS.. Talanta, 2011, 83 (5), pp.1769-1773. ?10.1016/j.talanta.2010.10.030?. ?hal-00591902?
  • Emmanuelle Vulliet, Cécile Cren-Olivé. Screening of pharmaceuticals and hormones at regional scale, in surface and groundwaters intended to human consumption. Environmental Pollution, 2011, 159 (10), pp.2929-2934. ?10.1016/j.envpol.2011.04.033?. ?hal-00616322?
  • Angélique Lazartigues, Laure Wiest, Robert Baudot, Marielle Thomas, Cyril Feidt, et al.. Multiresidue method to quantify pesticides in fish muscle by QuEChERS-based extraction and LC-MS/MS. Analytical and Bioanalytical Chemistry, 2011, 400 (7), pp.2185-2193. ?10.1007/s00216-011-4945-z?. ?hal-00616317?